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Dalton: Found 47 synthesis runs above 400 °C. Capacity plateaus past 430 °C. XRD from runs #31–34 shows a secondary phase flagged as noise. Suggest re-running #33 at 415 °C with slower ramp.
| Run | Date | Temp | Capacity | Status |
|---|---|---|---|---|
| #29 | Jun 02 | 405 °C | 182 mAh/g | Complete |
| #31 | Jun 09 | 428 °C | 171 mAh/g | Anomaly |
| #33 | Jun 14 | 431 °C | 168 mAh/g | Anomaly |
| #36 | Jun 21 | 415 °C | – | Proposed |